If you mean dual-booting, yes it can be done, but it's a bit fiddly - the XP bootloader will stamp all over the Vista version and then fail to recognise the existing Vista installation, so you'll have to reconfigure things manually.
There's a guide here which seems to explain it nicely.
Unless you need your full hardware capabilities under XP, it might be better to install it as a guest in a virtual machine.
Have 2 laptops in the house on Vista,also another pc on Vista but my media centre pc i would prefer to have on XP. The media pc i connect to work with as it uses a vpn client that Vista causes issues with.
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